trans-Pd(COPh)I(PMe₃)2

Base Information

Chemical Name:trans-Pd(COPh)I(PMe₃)2
CAS No.:68391-85-5
Molecular Formula:C₁₃H₂₃IOP₂Pd
Molecular Weight:490.597
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-Pd(COPh)I(PMe₃)2

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Technology Process of trans-Pd(COPh)I(PMe₃)2

There total 2 articles about trans-Pd(COPh)I(PMe₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 50417-71-5
trans-Pd(COPh)I(PPh₃)2

: 594-09-2
trimethylphosphane

: 68391-85-5
trans-Pd(COPh)I(PMe₃)2

Guidance literature:: In dichloromethane; phosphine was added to heterogenous mixture of trans-benzoyl complex and CH2Cl2 under N2 at -30°C, mixture was stirred at room temp. to turn into a homogenous red soln., the latter was concd., hexane was added, the ppt. was filtered; purified by column chromatography; identified by elem. anal. and IR spectrum;

Reference yield:

: trans-{PdI(Ph)(PMe₃)2}

: 68391-85-5
trans-Pd(COPh)I(PMe₃)2

Guidance literature:: With carbon monoxide; In methanol; triethylamine; Pd-complex was reacted with CO at 25°C in MeOH-Et3N; characterized by (1)H, (31)P NMR and IR spectra and elem. anal.;
DOI:10.1039/c39860000817