N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

Base Information

• Chemical Name: N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide
• CAS No.: 181786-38-9
• Molecular Formula: C₃₄H₃₈N₄O₅Si
• Molecular Weight: 610.785

Synonyms:

Chemical Property of N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

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Technology Process of N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

There total 1 articles about N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (3aR,6R,6aS)-6-(tert-butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl ester → N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide (181786-38-9) + N-{1-[(3aR,4R,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide (181632-01-9)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; silylated N⁴-benzoylated cytosine; In dichloromethane; for 12h; Product distribution; Ambient temperature; other solvent;

DOI:10.1016/S0960-894X(96)00262-4

Reference yield:

N-{1-[(3aR,4S,6R,6aS)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide (181786-38-9) → N-[1-((3aR,4S,6R,6aS)-6-Hydroxymethyl-2-methyl-hexahydro-furo[3,4-d]isoxazol-4-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-benzamide

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; water; for 0.5h; Ambient temperature;

DOI:10.1016/S0960-894X(96)00262-4

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