Technology Process of C24H35F2N5O
There total 6 articles about C24H35F2N5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane
2: sodium tris(acetoxy)borohydride / dichloromethane
With
sodium tris(acetoxy)borohydride; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.bmcl.2010.12.118
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dichloromethane / Molecular sieve
2: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 2068.65 Torr
3: O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
4: trifluoroacetic acid / dichloromethane
5: sodium tris(acetoxy)borohydride / dichloromethane
With
palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.118
- Guidance literature:
-
Multi-step reaction with 3 steps
1: O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
2: trifluoroacetic acid / dichloromethane
3: sodium tris(acetoxy)borohydride / dichloromethane
With
sodium tris(acetoxy)borohydride; O-(1,2-dihydro-2-oxo-1-pyridyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.118