p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

Base Information

Chemical Name:p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine
CAS No.:81224-26-2
Molecular Formula:C₁₉H₁₉ClN₂O₂
Molecular Weight:342.825
Hs Code.:

Synonyms:

Suppliers and Price of p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

There total 8 articles about p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-57-4
2-bromoanisole

: 81224-26-2
p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / AlCl₃ / CH₂Cl₂ / 0.33 h / 0 °C

2: 88 percent / p-TsOH / benzene / 40 h / Heating

3: 1) n-BuLi / 1) ether, -20 deg C, 4 h , 2) RT, 12 h

4: CH₃ONa / methanol / 5 h / 0 °C

5: xylene / 3 h / Heating

6: 93 percent / aq. KOH / 0.5 h / Heating

7: 77 percent / copper chromite (barium promoted) / quinoline / 7 h / 190 °C

8: 65 percent / methanol / 96 h / Heating

With n-butyllithium; aluminium trichloride; sodium methylate; toluene-4-sulfonic acid; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; dichloromethane; xylene; benzene;

Reference yield:

: 81224-20-6
(3-bromo-4-methoxyphenyl)(4-chlorophenyl)methanone

: 81224-26-2
p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / p-TsOH / benzene / 40 h / Heating

2: 1) n-BuLi / 1) ether, -20 deg C, 4 h , 2) RT, 12 h

3: CH₃ONa / methanol / 5 h / 0 °C

4: xylene / 3 h / Heating

5: 93 percent / aq. KOH / 0.5 h / Heating

6: 77 percent / copper chromite (barium promoted) / quinoline / 7 h / 190 °C

7: 65 percent / methanol / 96 h / Heating

With n-butyllithium; sodium methylate; toluene-4-sulfonic acid; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; xylene; benzene;

Reference yield:

: 81224-22-8
p-chlorobenzoyl-5 methoxy-2 benzaldehyde

: 81224-26-2
p-chlorobenzoyl-7 methoxy-4 N,N-dimethylgramine

Guidance literature:: Multi-step reaction with 5 steps

1: CH₃ONa / methanol / 5 h / 0 °C

2: xylene / 3 h / Heating

3: 93 percent / aq. KOH / 0.5 h / Heating

4: 77 percent / copper chromite (barium promoted) / quinoline / 7 h / 190 °C

5: 65 percent / methanol / 96 h / Heating

With sodium methylate; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; xylene;