C₂₇H₂₃⁽¹⁸⁾FN₄O₃

Base Information

Chemical Name:C₂₇H₂₃⁽¹⁸⁾FN₄O₃
CAS No.:1353016-74-6
Molecular Formula:C₂₇H₂₃FN₄O₃
Molecular Weight:469.505
Hs Code.:

C<sub>27</sub>H<sub>23</sub><sup>(18)</sup>FN<sub>4</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₃⁽¹⁸⁾FN₄O₃

Chemical Property:

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Technology Process of C₂₇H₂₃⁽¹⁸⁾FN₄O₃

There total 8 articles about C₂₇H₂₃⁽¹⁸⁾FN₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1021-91-6
N-[tricyclo[9.4.0.0^3,8]pentadeca-1⁽¹¹⁾,3,5,7,9,12,14-heptaen-2-ylidene]hydroxylamine

: 1353016-74-6
C₂₇H₂₃⁽¹⁸⁾FN₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1: 1,3,5-trichloro-2,4,6-triazine; N,N-dimethyl-formamide / 20 °C

2: diisobutylaluminium hydride / dichloromethane / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4: bromine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5: potassium tert-butylate / tetrahydrofuran / 4 h / -40 °C / Inert atmosphere

6: dimethyl sulfoxide / 0.25 h / 37 °C / Human plasma

With 1,3,5-trichloro-2,4,6-triazine; potassium tert-butylate; bromine; diisobutylaluminium hydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1: Beckmann rearrangement;
DOI:10.1002/anie.201105547

Reference yield:

: 17271-88-4
p-nitrobenzyl azide

: 1353016-74-6
C₂₇H₂₃⁽¹⁸⁾FN₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1: [¹⁸F]-potassium fluoride / acetonitrile / 110 °C

2: dimethyl sulfoxide / 0.25 h / 37 °C / Human plasma

With [¹⁸F]-potassium fluoride; In dimethyl sulfoxide; acetonitrile;
DOI:10.1002/anie.201105547

Reference yield:

: 2222-33-5
dibenzosuberenon

: 1353016-74-6
C₂₇H₂₃⁽¹⁸⁾FN₄O₃

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine; hydroxylamine hydrochloride / ethanol / 3 h / Reflux

2: 1,3,5-trichloro-2,4,6-triazine; N,N-dimethyl-formamide / 20 °C

3: diisobutylaluminium hydride / dichloromethane / 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

5: bromine / dichloromethane / 1 h / 0 °C / Inert atmosphere

6: potassium tert-butylate / tetrahydrofuran / 4 h / -40 °C / Inert atmosphere

7: dimethyl sulfoxide / 0.25 h / 37 °C / Human plasma

With pyridine; 1,3,5-trichloro-2,4,6-triazine; hydroxylamine hydrochloride; potassium tert-butylate; bromine; diisobutylaluminium hydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; 2: Beckmann rearrangement;
DOI:10.1002/anie.201105547