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Technology Process of bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate

bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate

Base Information
  • Chemical Name:bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate
  • CAS No.:75812-23-6
  • Molecular Formula:C49H35BrFeO3P*F6P
  • Molecular Weight:983.504
  • Hs Code.:
bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate

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Chemical Property of bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate
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Technology Process of bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate

There total 1 articles about bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

[Fe(CO)2(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>5</sub>(C<sub>6</sub>H<sub>5</sub>)4OAg)]2<sup>(2+)</sup>*2PF<sub>6</sub><sup>(1-)</sup>=[Fe(CO)2(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>5</sub>(C<sub>6</sub>H<sub>5</sub>)4O)Ag]2(PF<sub>6</sub>)2

[Fe(CO)2(P(C6H5)3)(C5(C6H5)4OAg)]2(2+)*2PF6(1-)=[Fe(CO)2(P(C6H5)3)(C5(C6H5)4O)Ag]2(PF6)2

silver(I) bromide

silver(I) bromide

bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate
75812-23-6

bromo(dicarbonyl)(η4-tetraphenylcyclopentadienone)(triphenylphosphine)iron hexafluorophosphate

Guidance literature:
With Br2; In dichloromethane; under N2; pptd. AgBr filtered off, filtrate reduced in vol., solid pptd. by addn.of hexane; elem. anal.;
DOI:10.1039/DT9800001710
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