Technology Process of C17H17NO5
There total 7 articles about C17H17NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[bis(acetoxy)iodo]benzene; potassium hydroxide;
In
formic acid;
at 0 ℃;
for 5h;
DOI:10.1021/ja408034x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; N,N-dimethyl-formamide / 27 h / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 1.66 h / 20 °C
3: dihydrogen peroxide; potassium carbonate / water; dimethyl sulfoxide / 4 h / 20 °C
4: [bis(acetoxy)iodo]benzene; potassium hydroxide / formic acid / 5 h / 0 °C
With
[bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium carbonate; potassium hydroxide;
In
formic acid; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja408034x
- Guidance literature:
-
Multi-step reaction with 5 steps
1: [bis(acetoxy)iodo]benzene / methanol / 0 °C
2: water; N,N-dimethyl-formamide / 27 h / 0 - 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 1.66 h / 20 °C
4: dihydrogen peroxide; potassium carbonate / water; dimethyl sulfoxide / 4 h / 20 °C
5: [bis(acetoxy)iodo]benzene; potassium hydroxide / formic acid / 5 h / 0 °C
With
[bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium carbonate; potassium hydroxide;
In
methanol; formic acid; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja408034x
