(1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol

Base Information

Chemical Name:(1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol
CAS No.:179091-13-5
Molecular Formula:C₁₁H₁₃ClO
Molecular Weight:196.677
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol

There total 7 articles about (1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1504-55-8,39924-63-5,55131-20-9
(E)-3-phenyl-2-methyl-2-propenol

: 179091-13-5
(1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol

Guidance literature:: Multi-step reaction with 6 steps

1: CSA

2: 50percent aq. NaOH / BTEAC

3: MeOH, PTS

4: 1.) Bu₃SnH, 2.) 10percent aq. KF / 1.) Et₃B / 1.) hexane, benzene, r.t., 20 h, 2.) 1 h

5: Jones' reagent

6: LiAlH₄ / tetrahydrofuran / Ambient temperature

With methanol; potassium fluoride; sodium hydroxide; lithium aluminium tetrahydride; jones' reagent; tri-n-butyl-tin hydride; pyridinium p-toluenesulfonate; triethyl borane; camphor-10-sulfonic acid; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran;
DOI:10.1039/P19960001243

Reference yield:

: [(1RS,3SR)-2,2-dichloro-1-methyl-3-phenylcyclopropyl]methanol

: 179091-13-5
(1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Bu₃SnH, 2.) 10percent aq. KF / 1.) Et₃B / 1.) hexane, benzene, r.t., 20 h, 2.) 1 h

2: Jones' reagent

3: LiAlH₄ / tetrahydrofuran / Ambient temperature

With potassium fluoride; lithium aluminium tetrahydride; jones' reagent; tri-n-butyl-tin hydride; triethyl borane; In tetrahydrofuran;
DOI:10.1039/P19960001243

Reference yield:

: 77301-62-3
(E)-2-Methyl-3-phenyl-2-propen-1-ol-tetrahydro-2-pyranylether

: 179091-13-5
(1S,2R,3R)-(+)-2-Chloro-1-methyl-3-phenylcyclopropylmethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 50percent aq. NaOH / BTEAC

2: MeOH, PTS

3: 1.) Bu₃SnH, 2.) 10percent aq. KF / 1.) Et₃B / 1.) hexane, benzene, r.t., 20 h, 2.) 1 h

4: Jones' reagent

5: LiAlH₄ / tetrahydrofuran / Ambient temperature

With methanol; potassium fluoride; sodium hydroxide; lithium aluminium tetrahydride; jones' reagent; tri-n-butyl-tin hydride; pyridinium p-toluenesulfonate; triethyl borane; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran;
DOI:10.1039/P19960001243