2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid

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Chemical Name:2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid
CAS No.:1053242-06-0
Molecular Formula:C₄₃H₃₉FeN₅O₈
Molecular Weight:809.658
Hs Code.:

2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid

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Chemical Property of 2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid

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Technology Process of 2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid

There total 1 articles about 2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 913745-70-7
tert-butyl-2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetate

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 1053242-06-0
2-(N-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)-2-(5-(N-ferrocenylbenzamido)-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetamido)acetic acid

Guidance literature:: With sodium hydroxide; sodium hydrogencarbonate; citric acid; In water; acetone; stirring iron complex in a mixt. of aq. NaOH and acetone for 5 h at roomtemp., addn. of aq. citric acid, addn. of aq. NaHCO3 until pH 8, addn. of water and acetone, addn. of fluorenyl compd., stirring for 24 h at ro om temp., addn. of aq. citric acid; evapn. of acetone, extn. with CH2Cl2, drying with na2SO4, filtration, evapn., column chromy. (silica, hexane/ethyl acetate 1:1 to acetone/water 5:1), evapn., dissolving in ethyl acetate, washing with water, drying with Na2SO4, filtration, evapn.;
DOI:10.1016/j.jorganchem.2008.05.009