Technology Process of C62H74O10
There total 4 articles about C62H74O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; potassium iodide;
In
acetone;
for 12h;
Reflux;
DOI:10.1039/c2jm30943b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetone / 6 h / Reflux
2: potassium carbonate; potassium iodide / acetone / 12 h / Reflux
With
potassium carbonate; potassium iodide;
In
acetone;
DOI:10.1039/c2jm30943b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide / methanol / Cooling with ice
1.2: 18 h / Reflux
2.1: boron trifluoride diethyl etherate / 4 h / 70 - 75 °C / Inert atmosphere
2.2: 1 h / 20 - 50 °C / Inert atmosphere
2.3: 1.5 h / 75 - 80 °C / Inert atmosphere
3.1: potassium carbonate / acetone / 6 h / Reflux
4.1: potassium carbonate; potassium iodide / acetone / 12 h / Reflux
With
boron trifluoride diethyl etherate; potassium carbonate; potassium iodide; potassium hydroxide;
In
methanol; acetone;
DOI:10.1039/c2jm30943b