trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone

Base Information

Chemical Name:trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone
CAS No.:81121-13-3
Molecular Formula:C₁₉H₂₀N₂O₂S
Molecular Weight:340.446
Hs Code.:

trans-β-<syn-9-bicyclo<4.2.1>nona-2,4,7-trienyl>acrolein tosylhydrazone

Synonyms:

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Chemical Property of trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone

Chemical Property:

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Technology Process of trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone

There total 6 articles about trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 81121-09-7
trans-β-nona-2,4,6-trienyl>acrolein tosylhydrazone

: 81176-69-4
C₁₉H₂₀N₂O₂S

: 81121-13-3
trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone

Guidance literature:: In chloroform; Title compound not separated from byproducts; Heating;
DOI:10.1021/jo00134a017

Reference yield:

: 28860-69-7
bicyclo<6.1.0>nona-2,4,6-triene-9-carboxaldehyde

: 81121-13-3
trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

2: 84 percent / glacial acetic acid / ethanol; bis-(2-methoxy-ethyl) ether / 0.28 h

3: 49 percent / CHCl₃ / Heating

With acetic acid; In ethanol; chloroform; diethylene glycol dimethyl ether;
DOI:10.1021/jo00134a017

Reference yield:

: 13380-66-0
9-(hydroxymethyl)bicyclo<6.1.0>nona-2,4,6-triene

: 81121-13-3
trans-β-nona-2,4,7-trienyl>acrolein tosylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 75.3 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h

3: 84 percent / glacial acetic acid / ethanol; bis-(2-methoxy-ethyl) ether / 0.28 h

4: 49 percent / CHCl₃ / Heating

With pyridine; chromium(VI) oxide; acetic acid; In ethanol; dichloromethane; chloroform; diethylene glycol dimethyl ether;
DOI:10.1021/jo00134a017