Technology Process of C38H46O9SSi
There total 6 articles about C38H46O9SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c2cc37099a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 0 - 20 °C / Inert atmosphere
2: CSA / acetonitrile / 1 h / 20 °C / Inert atmosphere
3: triethylamine; dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere
4: hydrogenchloride / ethyl acetate; water / 0.5 h / 0 °C / Inert atmosphere
5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
1H-imidazole; hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc37099a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 2.5 h / 0 - 20 °C / Inert atmosphere
2: CSA / acetonitrile / 1 h / 20 °C / Inert atmosphere
3: triethylamine; dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere
4: hydrogenchloride / ethyl acetate; water / 0.5 h / 0 °C / Inert atmosphere
5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
With
1H-imidazole; hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc37099a