Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

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Chemical Name:Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid
CAS No.:115523-63-2
Molecular Formula:C₅₈H₇₈N₂O₁₆Si₂
Molecular Weight:1115.43
Hs Code.:

Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

There total 4 articles about Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 115523-63-2
Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h

2: 48 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / Ambient temperature

3: 4-dimethylaminopyridine / pyridine / 2 h

With dmap; toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90840-1

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 115523-63-2
Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dioxane; H₂O / 6 h

2: pyridine / 3 h

3: 48 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / Ambient temperature

4: 4-dimethylaminopyridine / pyridine / 2 h

With dmap; potassium carbonate; toluene-4-sulfonic acid; In 1,4-dioxane; pyridine; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90840-1

Reference yield:

: 92054-17-6
Benzyl-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-6-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-glucopyranosid

: 115523-63-2
Benzyl-4-O-acetyl-6-O-<6-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-3,4-O-(tetraisopropyldisiloxan-1,3-diyl)-β-D-glucopyranosyl>-3-O-benzyl-2-benzyloxycarbonylamino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 1 M NaOMe; 2.) 80 percent hydrazine / 1.) methanol, 45 min; 2.) ethanol, 100 deg C, 2 h

2: K₂CO₃ / dioxane; H₂O / 6 h

3: pyridine / 3 h

4: 48 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / Ambient temperature

5: 4-dimethylaminopyridine / pyridine / 2 h

With dmap; sodium methylate; potassium carbonate; hydrazine hydrate; toluene-4-sulfonic acid; In 1,4-dioxane; pyridine; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90840-1