C₆H₄O₂BOC(C₆H₅)CHC(CH₃)N(C₄H₉)

Base Information

• Chemical Name: C₆H₄O₂BOC(C₆H₅)CHC(CH₃)N(C₄H₉)
• CAS No.: 102696-45-7
• Molecular Formula: C₂₀H₂₂BNO₃
• Molecular Weight: 335.211
• Mol file: 102696-45-7.mol

Synonyms:

Chemical Property of C₆H₄O₂BOC(C₆H₅)CHC(CH₃)N(C₄H₉)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₆H₄O₂BOC(C₆H₅)CHC(CH₃)N(C₄H₉)

There total 1 articles about C₆H₄O₂BOC(C₆H₅)CHC(CH₃)N(C₄H₉) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2-isopropoxy-1,3,2-benzodioxaborole (61676-63-9) + 1-phenyl-3-(butylamino)but-2-en-1-one (76943-80-1) → C6H4O2BOC(C6H5)CHC(CH3)N(C4H9) (102696-45-7)

Guidance literature:

In benzene; byproducts: (CH3)2CHOH; addn. of β-ketoamine to a soln. of benzodioxaborole in benzene, refluxing, fractionating azeotropically 2-propanol with benzene over a period of 8 h, progress of reaction is followed by estimation of 2-propanol in the azeotrope; removal of excess of solvent under reduced pressure, recrystn. from benzene/n-hexane mixt., elem. anal.;

upstream raw materials:

2-isopropoxy-1,3,2-benzodioxaborole

1-phenyl-3-(butylamino)but-2-en-1-one