(+)-pinoresinol monomethyl ether

Base Information

• Chemical Name: (+)-pinoresinol monomethyl ether
• CAS No.: 23487-12-9
• Molecular Formula: C₂₁H₂₄O₆
• Molecular Weight: 372.418

Synonyms:

Chemical Property of (+)-pinoresinol monomethyl ether

Chemical Property:

Purity/Quality:

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Technology Process of (+)-pinoresinol monomethyl ether

There total 9 articles about (+)-pinoresinol monomethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

eudesmine (526-06-7,4375-03-5,16499-02-8,25305-05-9,29106-36-3,38609-26-6,38759-91-0,60102-89-8) → (-)-pinoresinol (81446-29-9) + (+)-pinoresinol monomethyl ether (487-39-8,23397-46-8,23397-47-9,23487-12-9,95404-51-6,29395-87-7) + methylpinoresinol

Guidance literature:

With dipotassium hydrogenphosphate; polypeptone; D-glucose; potassium chloride; magnesium sulfate; iron(II) sulfate; Sucrose; In water; dimethyl sulfoxide; at 25 ℃; for 72h; Yields of byproduct given; Aspergillus niger IFO 4414 presence;

DOI:10.1016/S0031-9422(96)00754-6

Reference yield: 14.1%

(+/-)-dimethylpinoresinol (526-06-7,4375-03-5,16499-02-8,25305-05-9,29106-36-3,38609-26-6,38759-91-0,60102-89-8) → (-)-pinoresinol (81446-29-9) + (+)-pinoresinol monomethyl ether (487-39-8,23397-46-8,23397-47-9,23487-12-9,95404-51-6,29395-87-7) + methylpinoresinol

Guidance literature:

With dipotassium hydrogenphosphate; polypeptone; D-glucose; potassium chloride; magnesium sulfate; iron(II) sulfate; Sucrose; In water; dimethyl sulfoxide; at 25 ℃; for 72h; Yields of byproduct given; Aspergillus niger IFO 4414 presence;

DOI:10.1016/S0031-9422(96)00754-6

Reference yield:

eudesmin (526-06-7,4375-03-5,16499-02-8,25305-05-9,29106-36-3,38609-26-6,38759-91-0,60102-89-8) → pinoresinol (4263-88-1,7452-03-1,10061-38-8,18779-41-4,18779-51-6,24404-50-0,81446-29-9,146338-76-3,487-36-5) + (+)-pinoresinol monomethyl ether (487-39-8,23397-46-8,23397-47-9,23487-12-9,95404-51-6,29395-87-7)

Guidance literature:

In dimethyl sulfoxide; for 24h; biotransformation by aspergillus niger;

DOI:10.1016/S0031-9422(00)90836-7

upstream raw materials:

(3R,4S,5S,6R)-2-{4-[(1S,3aR,4S,6aR)-4-(3,4-Dimethoxy-phenyl)-tetrahydro-furo[3,4-c]furan-1-yl]-2-methoxy-phenoxy}-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

eudesmin

eudesmine

(+/-)-dimethylpinoresinol

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