C₂₇H₃₀N₂O₅S

Base Information

Chemical Name:C₂₇H₃₀N₂O₅S
CAS No.:1360744-17-7
Molecular Formula:C₂₇H₃₀N₂O₅S
Molecular Weight:494.612
Hs Code.:

C<sub>27</sub>H<sub>30</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₇H₃₀N₂O₅S

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Technology Process of C₂₇H₃₀N₂O₅S

There total 16 articles about C₂₇H₃₀N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360744-14-4
C₂₇H₃₂N₂O₅S

: 1360744-17-7
C₂₇H₃₀N₂O₅S

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-09-7
C₁₂H₁₈O₄

: 1360744-17-7
C₂₇H₃₀N₂O₅S

Guidance literature:: Multi-step reaction with 14 steps

1.1: hydrogen iodide / water; toluene / 0.5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

4.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

5.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

5.2: 1 h / 0 - 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

6.2: 3 h / 20 °C

7.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

8.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

9.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

10.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

11.1: triethylamine / dichloromethane / 10 h

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran

13.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / -78 °C / Reflux

14.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / -78 °C

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen iodide; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: Sonogashira coupling / 5.1: Hydroboration reaction / 7.1: Barton-McCombie deoxygenation / 9.1: Wittig reaction / 14.1: Swern oxidation;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-08-6
C₂₃H₂₇IO₂Si

: 1360744-17-7
C₂₇H₃₀N₂O₅S

Guidance literature:: Multi-step reaction with 12 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

2.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

3.2: 1 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

4.2: 3 h / 20 °C

5.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

7.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

8.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

9.1: triethylamine / dichloromethane / 10 h

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / -78 °C / Reflux

12.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / -78 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 1.1: Sonogashira coupling / 3.1: Hydroboration reaction / 5.1: Barton-McCombie deoxygenation / 7.1: Wittig reaction / 12.1: Swern oxidation;
DOI:10.1002/chem.201102101