C₅₂H₅₆N₂O₁₂

Base Information

Chemical Name:C₅₂H₅₆N₂O₁₂
CAS No.:1361416-96-7
Molecular Formula:C₅₂H₅₆N₂O₁₂
Molecular Weight:901.023
Hs Code.:

C<sub>52</sub>H<sub>56</sub>N<sub>2</sub>O<sub>12</sub>

Synonyms:

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Chemical Property of C₅₂H₅₆N₂O₁₂

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Technology Process of C₅₂H₅₆N₂O₁₂

There total 6 articles about C₅₂H₅₆N₂O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1361417-02-8
C₆₂H₇₂N₂O₁₆

: 1361416-96-7
C₅₂H₅₆N₂O₁₂

Guidance literature:: With chloro-trimethyl-silane; phenol; In dichloromethane; for 14h;
DOI:10.3762/bjoc.7.184

Reference yield:

: 82684-68-2
1,4-bis[4-(carbonochloridoyl)phenyl] benzene-1,4-dicarboxylate

: 1361416-96-7
C₅₂H₅₆N₂O₁₂

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / -4 - 20 °C

2: tetramethyl ammoniumhydroxide; sodium iodide / dimethyl sulfoxide / 2 h / 60 °C

3: chloro-trimethyl-silane; phenol / dichloromethane / 14 h

With pyridine; chloro-trimethyl-silane; tetramethyl ammoniumhydroxide; sodium iodide; phenol; In dichloromethane; dimethyl sulfoxide;
DOI:10.3762/bjoc.7.184

Reference yield:

: 100-20-9
terephthaloyl chloride

: 1361416-96-7
C₅₂H₅₆N₂O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water; 1,2-dichloro-ethane / 5 h / 5 - 20 °C

2: thionyl chloride / 4 h / Reflux

3: pyridine / dichloromethane / -4 - 20 °C

4: tetramethyl ammoniumhydroxide; sodium iodide / dimethyl sulfoxide / 2 h / 60 °C

5: chloro-trimethyl-silane; phenol / dichloromethane / 14 h

With pyridine; chloro-trimethyl-silane; thionyl chloride; tetramethyl ammoniumhydroxide; sodium iodide; sodium hydroxide; phenol; In dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.3762/bjoc.7.184