anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine

Base Information

Chemical Name:anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine
CAS No.:1262488-40-3
Molecular Formula:C₃₈H₃₈B₂N₂O₄
Molecular Weight:608.353
Hs Code.:

Synonyms:

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Chemical Property of anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine

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Technology Process of anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine

There total 8 articles about anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.5%

: 1262488-46-9
(4-([(anthracen-9-ylmethyl)-amino]-methyl)-benzyl)-methyl-amine

: 174900-86-8
propane-1,3-diyl(o-(bromomethyl)phenyl)boronate

: 1262488-40-3
anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine

Guidance literature:: With K₂CO₃; In acetonitrile; dioxaborinane and K2CO3 successively added to soln. of diamine in MeCN under stirring, mixt. refluxed for 5 h; evapn. under vac., water added, extn. with CH2Cl2, org. phase dried overMgSO4, filtered, filtrate evapd. under vac., recrystn. from CHCl3/hexan e;
DOI:10.1039/c0nj00578a

Reference yield:

: C₂₄H₂₂N₂

: 1262488-40-3
anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 4 h / 20 °C

2: potassium carbonate / acetonitrile / 5 h / Reflux

With sodium tetrahydroborate; potassium carbonate; In methanol; acetonitrile;
DOI:10.1039/c0nj00578a

Reference yield:

: 31417-69-3
1-(4-(aminomethyl)phenyl)-N-methylmethanamine

: 1262488-40-3
anthracen-9-ylmethyl-(2-boronobenzyl)-(4-([(2-boronobenzyl)-methyl-amino]methyl)-benzyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 5 h / 20 °C

2: sodium tetrahydroborate / methanol / 4 h / 20 °C

3: potassium carbonate / acetonitrile / 5 h / Reflux

With sodium tetrahydroborate; potassium carbonate; In methanol; acetonitrile;
DOI:10.1039/c0nj00578a