Technology Process of C21H32O5S
There total 7 articles about C21H32O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1H-imidazole; dmap
2: dimethylsulfide borane complex; dihydrogen peroxide; sodium hydroxide / tetrahydrofuran
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide
4: diethyl ether
5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide
6: dichloro bis(acetonitrile) palladium(II); oxygen; copper(l) chloride / water; N,N-dimethyl-formamide
7: triethylamine / dichloromethane
With
1H-imidazole; dmap; dichloro bis(acetonitrile) palladium(II); dimethylsulfide borane complex; dihydrogen peroxide; oxygen; triethylamine; copper(l) chloride; sodium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
6: Wacker oxidation;
DOI:10.1055/s-0030-1259081
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide
2: dichloro bis(acetonitrile) palladium(II); oxygen; copper(l) chloride / water; N,N-dimethyl-formamide
3: triethylamine / dichloromethane
With
dichloro bis(acetonitrile) palladium(II); oxygen; triethylamine; copper(l) chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
2: Wacker oxidation;
DOI:10.1055/s-0030-1259081