C₂₃H₃₆O₄

Base Information

Chemical Name:C₂₃H₃₆O₄
CAS No.:1351657-04-9
Molecular Formula:C₂₃H₃₆O₄
Molecular Weight:376.536
Hs Code.:

C<sub>23</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₃H₃₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₃H₃₆O₄

There total 15 articles about C₂₃H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80657-88-1
(2R,4R)-2-Methyl-4-((4S,5R)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-pentan-1-ol

: 1351657-04-9
C₂₃H₃₆O₄

Guidance literature:: Multi-step reaction with 9 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride / tetrahydrofuran

4: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

5: pyridine; tributylphosphine

6: dichloromethane

7: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

8: sodium periodate / methanol; water

9: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: Swern oxidation / 2: Horner-Emmons olefination / 4: Katsuki-Sharpless epoxidation / 9: Pummerer rearrangement;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: 1351656-96-6
C₁₄H₂₆O₄

: 1351657-04-9
C₂₃H₃₆O₄

Guidance literature:: Multi-step reaction with 10 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

3: sodium hydride / tetrahydrofuran

4: diisobutylaluminium hydride / tetrahydrofuran

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

6: pyridine; tributylphosphine

7: dichloromethane

8: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

9: sodium periodate / methanol; water

10: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 2: Swern oxidation / 3: Horner-Emmons olefination / 5: Katsuki-Sharpless epoxidation / 10: Pummerer rearrangement;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: C₁₃H₂₄O₃

: 1351657-04-9
C₂₃H₃₆O₄

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydride / tetrahydrofuran

2: diisobutylaluminium hydride / tetrahydrofuran

3: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

4: pyridine; tributylphosphine

5: dichloromethane

6: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

7: sodium periodate / methanol; water

8: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

With pyridine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; diethyl (2S,3S)-tartrate; tributylphosphine; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: Horner-Emmons olefination / 3: Katsuki-Sharpless epoxidation / 8: Pummerer rearrangement;
DOI:10.1016/j.tetlet.2011.10.073