(3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one

Base Information

Chemical Name:(3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one
CAS No.:107699-59-2
Molecular Formula:C₂₈H₃₀N₂O₃
Molecular Weight:442.558
Hs Code.:

(3RS,4RS) 4-<(<tetrahydropyran-2-yl>-oxy)-methyl> 3-tritylamino azetidin-2-one

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Chemical Property of (3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one

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Technology Process of (3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one

There total 3 articles about (3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 76-83-5
trityl chloride

: 766468-92-2,781574-86-5
(3RS,4RS) 3-amino 4(<(tetrahydropyran-2-yl)-oxy>-methyl) azetidin-2-one

: 107699-59-2,107795-33-5
(3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1016/S0040-4020(01)90553-8

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 107699-59-2,107795-33-5
(3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / p-toluenesulfonic acid / tetrahydrofuran / 20 h / 20 °C

2: hydrogen / 5percent Pd/C / ethanol / 0.25 h / 20 °C

3: 78 percent / triethylamine / CH₂Cl₂ / 6 h / 20 °C

With hydrogen; toluene-4-sulfonic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)90553-8

Reference yield:

: 107699-64-9,107795-34-6
(3RS,4RS) 3-(<(phenylmethyl)-oxy>-carbonyl)-amino 4-(<(tetrahydropyran-2-yl)-oxy>-methyl) azetidin-2-one

: 107699-59-2,107795-33-5
(3RS,4RS) 4-<(-oxy)-methyl> 3-tritylamino azetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 5percent Pd/C / ethanol / 0.25 h / 20 °C

2: 78 percent / triethylamine / CH₂Cl₂ / 6 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)90553-8