3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose

Base Information

• Chemical Name: 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose
• CAS No.: 79705-66-1
• Molecular Formula: C₆₀H₇₁NO₂₂
• Molecular Weight: 1158.22

Synonyms:

Chemical Property of 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose

There total 2 articles about 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

acetic anhydride (108-24-7) + 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-1,6-anhydro-2-O-benzyl-β-D-galactopyranose (79723-94-7) → 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-β-D-galactopyranose (79705-66-1,79733-89-4) + 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose (79705-66-1,79733-89-4)

Guidance literature:

With trifluoroacetic acid; for 24h; Ambient temperature;

Reference yield: 67.0%

acetic anhydride (108-24-7) + 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-1,6-anhydro-2-O-benzyl-β-D-galactopyranose (79723-94-7) → 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-β-D-galactopyranose (79705-66-1,79733-89-4) + 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranose (79705-66-1,79733-89-4)

Guidance literature:

With trifluoroacetic acid; for 24h; Ambient temperature;

Reference yield:

3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-1,6-di-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-D-galactopyranose (79705-66-1,79733-89-4) → 3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-6-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranosylbromid (79705-68-3)

Guidance literature:

With TiBr; In dichloromethane; ethyl acetate; at 0 ℃; for 16h; Yield given;

upstream raw materials:

acetic anhydride

3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-1,6-anhydro-2-O-benzyl-β-D-galactopyranose

Downstream raw materials:

3-O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-6-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranosylbromid

Benzyl-4-O-<3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-6-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

Benzyl-4-O-<3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-6-O-acetyl-4-O-(6-O-acetyl-2,3,4-tri-O-benzyl-β-D-mannopyranosyl)-2-O-benzyl-α-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

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