5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol

Base Information

Chemical Name:5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol
CAS No.:99875-45-3
Molecular Formula:C₁₆H₂₄O₂
Molecular Weight:248.365
Hs Code.:

Synonyms:

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Chemical Property of 5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol

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Technology Process of 5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol

There total 5 articles about 5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: phenylmagnesium bromide

: 99875-52-2
5(e)-(tert-Butyl)-3(a)-hydroxycyclohexanon

: 99875-45-3
5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol

Guidance literature:: In diethyl ether; at -40 - 25 ℃; for 1h;

Reference yield:

: 32360-28-4
5-tert-butylcyclohex-2-en-1-one

: 99875-45-3
5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / p-toluenesulfonic acid / toluene / 18 h / Heating

2: 48 percent / Hg(OCOCH₃)2, NaBH₄

3: 91 percent / p-toluenelsulfonic acid / acetonitrile; H₂O / 1 h / Ambient temperature

4: 15 percent / diethyl ether / 1 h / -40 - 25 °C

With sodium tetrahydroborate; mercury(II) diacetate; toluene-4-sulfonic acid; In diethyl ether; water; toluene; acetonitrile;

Reference yield:

: 32591-15-4
trans-5-tert-butylcyclohex-2-enol

: 99875-45-3
5(e)-(tert-Butyl)-1(e)-phenyl-1(a),3(a)-cyclohexandiol

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / Na₂Cr₂O₇*2H₂O, H₂SO₄ conc. / diethyl ether; H₂O / 1 h

2: 66 percent / p-toluenesulfonic acid / toluene / 18 h / Heating

3: 48 percent / Hg(OCOCH₃)2, NaBH₄

4: 91 percent / p-toluenelsulfonic acid / acetonitrile; H₂O / 1 h / Ambient temperature

5: 15 percent / diethyl ether / 1 h / -40 - 25 °C

With sodium tetrahydroborate; sodium dichromate; sulfuric acid; mercury(II) diacetate; toluene-4-sulfonic acid; In diethyl ether; water; toluene; acetonitrile;