C₅₃H₇₄N₁₀O₈S

Base Information

Chemical Name:C₅₃H₇₄N₁₀O₈S
CAS No.:1354551-63-5
Molecular Formula:C₅₃H₇₄N₁₀O₈S
Molecular Weight:1011.3
Hs Code.:

C<sub>53</sub>H<sub>74</sub>N<sub>10</sub>O<sub>8</sub>S

Synonyms:

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Chemical Property of C₅₃H₇₄N₁₀O₈S

Chemical Property:

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Technology Process of C₅₃H₇₄N₁₀O₈S

There total 11 articles about C₅₃H₇₄N₁₀O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872346-84-4
benzyl (3S,4S)-3-hydroxy-4-methyloctanoate

: 1354551-63-5
C₅₃H₇₄N₁₀O₈S

Guidance literature:: Multi-step reaction with 9 steps

1: dmap; diisopropyl-carbodiimide / dichloromethane; water / 30 h / 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

5: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

6: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

7: trimethylamine hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

8: sodium azide / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

9: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 10 h / 50 °C

With hydrogenchloride; dmap; sodium azide; 1-hydroxy-7-aza-benzotriazole; copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; hydrogen; trimethylamine hydrochloride; benzotriazol-1-ol; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; diisopropyl-carbodiimide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.10.045

Reference yield:

: 1354551-67-9
C₄₂H₅₃N₃O₈S

: 1354551-63-5
C₅₃H₇₄N₁₀O₈S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 10 h / 50 °C

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.10.045

Reference yield:

: 1354551-65-7
Boc-L-Dph-D-Ser-OBn

: 1354551-63-5
C₅₃H₇₄N₁₀O₈S

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

4: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

5: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

6: trimethylamine hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

7: sodium azide / N,N-dimethyl-formamide / 4 h / 50 °C / Inert atmosphere

8: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 10 h / 50 °C

With hydrogenchloride; sodium azide; 1-hydroxy-7-aza-benzotriazole; copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; hydrogen; trimethylamine hydrochloride; benzotriazol-1-ol; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.10.045