methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate

Base Information

• Chemical Name: methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate
• CAS No.: 911380-51-3
• Molecular Formula: C₂₈H₃₀O₇
• Molecular Weight: 478.542

Synonyms:

Chemical Property of methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate

Chemical Property:

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Technology Process of methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate

There total 2 articles about methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((3R,4S,5R,6S)-3,4,5-Tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-methanol (641635-63-4) → methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate (911380-51-3)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In acetone; at 0 - 20 ℃; for 1.16667h;

DOI:10.1055/s-2004-834889

Reference yield:

methyl 2,3,4-tri-O-benzyl-β-L-idopyranoside (205192-05-8,641635-63-4) → methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate (911380-51-3)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In acetone; at 0 ℃; for 0.166667h;

DOI:10.1002/chem.200600268

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + methyl 2,3,4-tri-O-benzyl-β-L-idopyranosiduronate (911380-51-3) → Methyl (methyl 2,3,4-tri-O-benzyl-β-L-idopyranoside)uronate (120567-49-9)

Guidance literature:

In diethyl ether; dichloromethane; at 0 ℃; for 1.5h;

DOI:10.1055/s-2004-834889

upstream raw materials:

((3R,4S,5R,6S)-3,4,5-Tris-benzyloxy-6-methoxy-tetrahydro-pyran-2-yl)-methanol

methyl 2,3,4-tri-O-benzyl-β-L-idopyranoside

Downstream raw materials:

Methyl (methyl 2,3,4-tri-O-benzyl-β-L-idopyranoside)uronate

dimethyl β-L-idopyranosiduronate

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