-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine

Chemical Name:(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine

CAS No.:74059-19-1
Molecular Formula:C₄₂H₄₅N₃O₃
Molecular Weight:639.838
Hs Code.:

(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo<a>quinolizine

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Chemical Property of (=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzoquinolizine

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Technology Process of (=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine

There total 5 articles about (=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 74059-18-0,106622-53-1
(+/-)-9-benzyloxy-N-<2-(5-benzyloxy-1H-indol-3-yl)ethyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine-2β-acetamide

: 74059-19-1,106550-20-3
(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine

Guidance literature:: With trichlorophosphate; In toluene; for 2.5h; Heating;
DOI:10.1248/cpb.33.3724

Reference yield:

: 20776-45-8
5-benzyloxytryptamine

: 74059-19-1,106550-20-3
(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 6 h / Ambient temperature

2: 69 percent / POCl₃ / toluene / 2.5 h / Heating

With diethyl cyanophosphonate; triethylamine; trichlorophosphate; In N,N-dimethyl-formamide; toluene;
DOI:10.1248/cpb.33.3724

Reference yield:

: 73053-54-0,73650-73-4
(+/-)-9-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine-2β-acetic acid

: 74059-19-1,106550-20-3
(=/-)-9-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-10-methoxy-2H-benzo quinolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / diethyl phosphorocyanidate, Et₃N / dimethylformamide / 6 h / Ambient temperature

2: 69 percent / POCl₃ / toluene / 2.5 h / Heating

With diethyl cyanophosphonate; triethylamine; trichlorophosphate; In N,N-dimethyl-formamide; toluene;
DOI:10.1248/cpb.33.3724