C₄₅H₆₈N₄O₇

Base Information

Chemical Name:C₄₅H₆₈N₄O₇
CAS No.:1009093-43-9
Molecular Formula:C₄₅H₆₈N₄O₇
Molecular Weight:777.058
Hs Code.:

C<sub>45</sub>H<sub>68</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:

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Chemical Property of C₄₅H₆₈N₄O₇

Chemical Property:

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Technology Process of C₄₅H₆₈N₄O₇

There total 12 articles about C₄₅H₆₈N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874348-11-5
(S)-N₁,N₁,4,4-tetramethylpentane-1,2-diamine

: 1009093-46-2
C₃₆H₄₈N₂O₈

: 1009093-43-9
C₄₅H₆₈N₄O₇

Guidance literature:: With HATU; In dichloromethane; at 23 ℃; for 2h;

Reference yield:

: 874347-50-9
C₈H₁₀INO₂

: 1009093-43-9
C₄₅H₆₈N₄O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: benzene / Heating / reflux

2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

2.2: 2 h

3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

4.2: 20 °C

4.3: 2 h

5.1: 4,6-bis(diphenylphosphanyl)phenoxathiine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 7 h / 80 °C

6.1: sodium periodate; ammonium acetate / water; acetone / 12 h / 23 °C

7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 5 h / 75 °C

8.1: HATU / dichloromethane / 2 h / 23 °C

With titanium(IV) isopropylate; sodium periodate; 4,6-bis(diphenylphosphanyl)phenoxathiine; ammonium acetate; trimethylaluminum; potassium acetate; caesium carbonate; pyridine hydrogenfluoride; HATU; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; pyridine; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; toluene; benzene;

Reference yield:

: 1009091-77-3
C₁₁H₁₂INO₄

: 1009093-43-9
C₄₅H₆₈N₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

1.2: 2 h

2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

3.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

3.2: 20 °C

3.3: 2 h

4.1: 4,6-bis(diphenylphosphanyl)phenoxathiine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 7 h / 80 °C

5.1: sodium periodate; ammonium acetate / water; acetone / 12 h / 23 °C

6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 5 h / 75 °C

7.1: HATU / dichloromethane / 2 h / 23 °C

With titanium(IV) isopropylate; sodium periodate; 4,6-bis(diphenylphosphanyl)phenoxathiine; ammonium acetate; trimethylaluminum; potassium acetate; caesium carbonate; pyridine hydrogenfluoride; HATU; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; pyridine; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; toluene;