C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O

Base Information

Chemical Name:C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O
CAS No.:915088-42-5
Molecular Formula:C₂₇H₃₀BN₃O₃
Molecular Weight:455.364
Hs Code.:

C<sub>6</sub>H<sub>5</sub>NNC<sub>6</sub>H<sub>4</sub>C(O)NHCH(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)BOC(CH<sub>3</sub>)2C(CH<sub>3</sub>)2O

Synonyms:

Suppliers and Price of C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O

There total 2 articles about C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 94242-84-9
4,4,5,5-tetramethyl-α-(phenylmethyl)-1,3,2-dioxaborolane-2-methanamine, trifluoroacetic acid salt

: 37790-20-8
(E)-4-(phenyldiazenyl)benzoic acid

: 915088-42-5
C₆H₅NNC₆H₄C(O)NHCH(CH₂C₆H₅)BOC(CH₃)2C(CH₃)2O

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; isobutylchloroformate added to soln. of 4-(phenylazo)benzoic acid in THF; NMM added; stirred for 10 min; soln. of B compd. in THF added; stirredfor 16 h; diluted with ethyl acetate; washed with H2O, brine; concd.; purifed by flash chromy. (EtOAc-CH2Cl2 3:7); >95% E isomer of B compd. obtained;
DOI:10.1039/b609320p