<amino>methylene>propanedioic acid diethyl ester

Base Information

Chemical Name:<amino>methylene>propanedioic acid diethyl ester
CAS No.:132844-57-6
Molecular Formula:C₂₃H₂₃F₃N₂O₄S
Molecular Weight:480.508
Hs Code.:

<<Cyclopropyl<6-(phenylthio)-5-(trifluoromethyl)-2-pyridinyl>amino>methylene>propanedioic acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <amino>methylene>propanedioic acid diethyl ester

Chemical Property:

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Technology Process of <amino>methylene>propanedioic acid diethyl ester

There total 1 articles about <amino>methylene>propanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 132844-57-6
<amino>methylene>propanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / methanol / 0.25 h / 0 °C

In methanol;
DOI:10.1002/jhet.5570270602

Reference yield: 45.0%

: 132844-57-6
<amino>methylene>propanedioic acid diethyl ester

: 132844-58-7
1-Cyclopropyl-1,4-dihydro-4-oxo-7-(phenylthio)-6-(trifluoromethyl)-1,8-naphthyridine-3-carboxylic acid ethyl ester

Guidance literature:: With sulfuric acid; acetic anhydride; for 0.5h;
DOI:10.1002/jhet.5570270602

Reference yield:

: 132844-57-6
<amino>methylene>propanedioic acid diethyl ester

: 132844-59-8
1-Cyclopropyl-1,4-dihydro-4-oxo-7-(phenylsulfonyl)-6-(trifluoromethyl)-1,8-naphthyridine-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Ac₂O, conc. H₂SO₄ / 0.5 h

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / 3.5 h / Heating

With sulfuric acid; acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/jhet.5570270602