2-methyl-1-phenylprop-1-enyl mercury bromide

Base Information

Chemical Name:2-methyl-1-phenylprop-1-enyl mercury bromide
CAS No.:122507-86-2
Molecular Formula:C₁₀H₁₁BrHg
Molecular Weight:411.691
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-1-phenylprop-1-enyl mercury bromide

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Technology Process of 2-methyl-1-phenylprop-1-enyl mercury bromide

There total 1 articles about 2-methyl-1-phenylprop-1-enyl mercury bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 5912-93-6
1-bromo-2-methyl-1-phenyl-1-propene

: mercury dibromide

: 122507-86-2
2-methyl-1-phenylprop-1-enyl mercury bromide

Guidance literature:: In tetrahydrofuran; vinyl bromide added to THF contg. Mg turnings until initiation occured, remainder of vinyl bromide added during 1h at reflux under N2, refluxed for further 1h, soln. transferred dropwise to soln. of HgBr2 at reflux, heated for 1h, stirred at room temp.; filtered, washed (THF), evapd., crystd. (cyclohexane/light petroleum); elem. anal.;
DOI:10.1039/P19880002847

Reference yield: 77.0%

: 122507-86-2
2-methyl-1-phenylprop-1-enyl mercury bromide

: 122507-79-3
bis(2-methyl-1-phenylprop-1-enyl)mercury

Guidance literature:: With potassium iodide; In water; acetone; soln. of KI in acetone and water added to soln. of Hg-compd. in acetone, pptn., stirred for 3h; collected, crystn. (light petroleum); elem. anal.;
DOI:10.1039/P19880002847