C₂₉H₃₃F₂N₃O₆

Base Information

Chemical Name:C₂₉H₃₃F₂N₃O₆
CAS No.:1416961-32-4
Molecular Formula:C₂₉H₃₃F₂N₃O₆
Molecular Weight:557.594
Hs Code.:

C<sub>29</sub>H<sub>33</sub>F<sub>2</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₉H₃₃F₂N₃O₆

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Technology Process of C₂₉H₃₃F₂N₃O₆

There total 13 articles about C₂₉H₃₃F₂N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1416960-83-2
1-benzyloxycarbonyl-(3R)-methoxy-(2R)-pyrrolidinemethanol

: 1416961-32-4
C₂₉H₃₃F₂N₃O₆

Guidance literature:: Multi-step reaction with 9 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 7 h / Reflux

2: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol / 22 h

3: Rh/Al₂O₃; trifluoroacetic acid; hydrogen / methanol / 15 h / 10?atm

4: sodium hydrogencarbonate / acetonitrile; water / 48 h / 20 °C

5: sodium ethanolate / ethanol / 16 h / Inert atmosphere; Reflux

6: potassium carbonate / 2 h / 60 °C

7: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

8: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 2 h / 20 °C

9: water; sodium hydroxide / tetrahydrofuran / 20 h / 20 °C

With di-isopropyl azodicarboxylate; 10 wt% Pd(OH)2 on carbon; Rh/Al₂O₃; water; hydrogen; sodium ethanolate; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2012.11.003

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 1416961-32-4
C₂₉H₃₃F₂N₃O₆

Guidance literature:: Multi-step reaction with 9 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 7 h / Reflux

2: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol / 22 h

3: Rh/Al₂O₃; trifluoroacetic acid; hydrogen / methanol / 15 h / 10?atm

4: sodium hydrogencarbonate / acetonitrile; water / 48 h / 20 °C

5: sodium ethanolate / ethanol / 16 h / Inert atmosphere; Reflux

6: potassium carbonate / 2 h / 60 °C

7: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

8: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 2 h / 20 °C

9: water; sodium hydroxide / tetrahydrofuran / 20 h / 20 °C

With di-isopropyl azodicarboxylate; 10 wt% Pd(OH)2 on carbon; Rh/Al₂O₃; water; hydrogen; sodium ethanolate; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2012.11.003

Reference yield:

: 1416960-84-3
ethyl 4-[(3R)-methoxy-(2R)-pyrrolidinylmethoxy]benzoate

: 1416961-32-4
C₂₉H₃₃F₂N₃O₆

Guidance literature:: Multi-step reaction with 7 steps

1: Rh/Al₂O₃; trifluoroacetic acid; hydrogen / methanol / 15 h / 10?atm

2: sodium hydrogencarbonate / acetonitrile; water / 48 h / 20 °C

3: sodium ethanolate / ethanol / 16 h / Inert atmosphere; Reflux

4: potassium carbonate / 2 h / 60 °C

5: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

6: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 2 h / 20 °C

7: water; sodium hydroxide / tetrahydrofuran / 20 h / 20 °C

With Rh/Al₂O₃; water; hydrogen; sodium ethanolate; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2012.11.003