3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one

Base Information

Chemical Name:3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one
CAS No.:131248-85-6
Molecular Formula:C₁₉H₁₃ClN₂OS
Molecular Weight:352.844
Hs Code.:

3-(p-chlorophenylthio)-1-methylbenzo<c><1,8>naphthyridin-6(5H)-one

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one

Chemical Property:

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Technology Process of 3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one

There total 3 articles about 3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 131248-86-7
3-chloro-1-methyl-6-(p-methylphenoxy)benzo<1,8>naphthyridine

: 106-54-7
p-Chlorothiophenol

: 131248-85-6
3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one

Guidance literature:: With water; In ethanol; for 2h; Heating;
DOI:10.1071/CH9901469

Reference yield:

: 106051-96-1
1-(p-methylphenoxy)isoquinoline-3-amine

: 131248-85-6
3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / acetic acid / 1.) 150 - 160 deg C, 1 h, 2.) reflux, 2 h

2: 67 percent / phosphoryl chloride / 0.33 h / Heating

3: 63 percent / H₂O / ethanol / 2 h / Heating

With water; acetic acid; trichlorophosphate; In ethanol;
DOI:10.1071/CH9901469

Reference yield:

: 131248-84-5
1-methyl-6-(p-methylphenoxy)benzo<1,8>naphthyridin-3(4H)-one

: 131248-85-6
3-(p-chlorophenylthio)-1-methylbenzo<1,8>naphthyridin-6(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / phosphoryl chloride / 0.33 h / Heating

2: 63 percent / H₂O / ethanol / 2 h / Heating

With water; trichlorophosphate; In ethanol;
DOI:10.1071/CH9901469