Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Base Information

Chemical Name:Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate
CAS No.:133961-11-2
Molecular Formula:C₂₄H₂₇N₂O₅S*Na
Molecular Weight:478.545
Hs Code.:

Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Chemical Property of Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Chemical Property:

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Technology Process of Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

There total 4 articles about Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2161-90-2
1-methoxy-1,3-cyclohexadiene

: 133961-11-2,134003-07-9
Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 25 percent / dichloromaleic acid, t-butyl-p-cresol / benzene / 504 h / 100 °C

2: KOH / ethanol; H₂O / 3 h / Heating

3: SOCl₂, EtN₃ / CH₂Cl₂ / -20 to -10 deg C

4: Et₃N / various solvent(s); H₂O / 0 deg C to r.t., 2 h

With potassium hydroxide; thionyl chloride; cis-2,3-dichlorobutenedioic acid; 2-tert-Butyl-4-methylphenol; triethylamine; ethyl azide; In ethanol; dichloromethane; water; benzene;
DOI:10.1039/P19910000651

Reference yield:

: 133961-10-1
(1R,2R,3S,4R)-1-Methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carboxylic acid

: 133961-11-2,134003-07-9
Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, EtN₃ / CH₂Cl₂ / -20 to -10 deg C

2: Et₃N / various solvent(s); H₂O / 0 deg C to r.t., 2 h

With thionyl chloride; triethylamine; ethyl azide; In dichloromethane; water;
DOI:10.1039/P19910000651

Reference yield:

: 133961-00-9
Ethyl (1RS,2RS,3SR,4RS)-1-methoxy-3-phenylbicyclo<2.2.2>oct-5-ene-2-carboxylate

: 133961-11-2,134003-07-9
Sodium; (2S,5R,6R)-6-[((1R,3S,4R)-1-methoxy-3-phenyl-bicyclo[2.2.2]oct-5-ene-2-carbonyl)-amino]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol; H₂O / 3 h / Heating

2: SOCl₂, EtN₃ / CH₂Cl₂ / -20 to -10 deg C

3: Et₃N / various solvent(s); H₂O / 0 deg C to r.t., 2 h

With potassium hydroxide; thionyl chloride; triethylamine; ethyl azide; In ethanol; dichloromethane; water;
DOI:10.1039/P19910000651