5-phenyl-2-methylphenylamino-4-oxazolinone

Base Information

• Chemical Name: 5-phenyl-2-methylphenylamino-4-oxazolinone
• CAS No.: 5841-16-7
• Molecular Formula: C₁₆H₁₄N₂O₂
• Molecular Weight: 266.299
• Mol file: 5841-16-7.mol

Synonyms:

Chemical Property of 5-phenyl-2-methylphenylamino-4-oxazolinone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-phenyl-2-methylphenylamino-4-oxazolinone

There total 2 articles about 5-phenyl-2-methylphenylamino-4-oxazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

5-phenyl-2-phenylimino-4-oxazolidinone (15900-36-4) + dimethyl sulfate (77-78-1) → 5-phenyl-2-methylphenylamino-4-oxazolinone (5841-16-7) + 5-phenyl-2-phenylimino-3-methyl-4-oxazolidinone (5841-17-8)

Guidance literature:

With sodium ethanolate; In ethanol; 1.) 1.5 h boiling, 2.) addition NaOEt and dimethyl sulfate, 1 h boiling;

DOI:10.1007/BF00472395

Reference yield:

sodium salt of 2-phenylpemoline + dimethyl sulfate (77-78-1) → 5-phenyl-2-methylphenylamino-4-oxazolinone (5841-16-7) + 5-phenyl-2-phenylimino-3-methyl-4-oxazolidinone (5841-17-8)

Guidance literature:

In ethanol; acetonitrile; Rate constant; Product distribution;

DOI:10.1007/BF00472395

upstream raw materials:

5-phenyl-2-phenylimino-4-oxazolidinone

dimethyl sulfate