C₂₄H₂₅N₇O₃

Base Information

Chemical Name:C₂₄H₂₅N₇O₃
CAS No.:1610767-00-4
Molecular Formula:C₂₄H₂₅N₇O₃
Molecular Weight:459.508
Hs Code.:

C<sub>24</sub>H<sub>25</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₄H₂₅N₇O₃

Chemical Property:

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Technology Process of C₂₄H₂₅N₇O₃

There total 10 articles about C₂₄H₂₅N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610766-97-6
(2R)-1-cyanobutan-2-yl[(1S)-1-{3-[N'-(4-cyano-3-methoxyphenyl)carbamimidamino]phenyl}ethyl] carbamate

: 19981-17-0,20611-81-8,123092-13-7,17292-62-5
sodium cyanamide

: 1610767-00-4
C₂₄H₂₅N₇O₃

Guidance literature:: (2R)-1-cyanobutan-2-yl[(1S)-1-{3-[N'-(4-cyano-3-methoxyphenyl)carbamimidamino]phenyl}ethyl] carbamate; With potassium carbonate; methyl iodide; In acetone; Inert atmosphere;

sodium cyanamide; In isopropyl alcohol; at 80 ℃; for 1h;
DOI:10.3109/14756366.2013.793184

Reference yield:

: 1610766-95-4
C₂₃H₂₅N₅O₃S

: 1610767-00-4
C₂₄H₂₅N₇O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; copper(II) sulfate; silica gel / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C

2.1: methyl iodide; potassium carbonate / acetone / Inert atmosphere

2.2: 1 h / 80 °C

With silica gel; potassium carbonate; copper(II) sulfate; triethylamine; methyl iodide; In tetrahydrofuran; acetone;
DOI:10.3109/14756366.2013.793184

Reference yield:

: 121-89-1
3-Nitroacetophenone

: 1610767-00-4
C₂₄H₂₅N₇O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

2.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / Inert atmosphere

3.1: triphenylphosphine / tetrahydrofuran; water / Inert atmosphere

4.1: D-tartaric acid / methanol / Inert atmosphere

4.2: Inert atmosphere

5.1: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / Inert atmosphere

6.1: ethyl acetate / 20 °C / Inert atmosphere

7.1: dichloromethane / 20 °C / Inert atmosphere

8.1: triethylamine; copper(II) sulfate; silica gel / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

8.2: 0.5 h / 20 °C

9.1: methyl iodide; potassium carbonate / acetone / Inert atmosphere

9.2: 1 h / 80 °C

With sodium tetrahydroborate; D-tartaric acid; diphenyl phosphoryl azide; 10 wt% Pd(OH)2 on carbon; hydrogen; silica gel; potassium carbonate; copper(II) sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; methyl iodide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; toluene;
DOI:10.3109/14756366.2013.793184