Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester

Base Information

Chemical Name:Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester
CAS No.:438569-49-4
Molecular Formula:C₂₈H₂₈O₃
Molecular Weight:412.529
Hs Code.:

Synonyms:

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Chemical Property of Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester

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Technology Process of Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester

There total 4 articles about Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 611-73-4
Benzoylformic acid

: 438569-49-4
Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dimethylformamide; CH₂Cl₂ / 2 h / 20 °C

2: 230 mg / pyridine / 12 h / 20 °C

With pyridine; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b109396g

Reference yield:

: 438569-45-0
2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-one

: 438569-49-4
Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / LAH / tetrahydrofuran / 2 h / 0 °C

2: 794 mg / 4-pyrrolidinopyridine; pyridine / toluene / 12 h / Heating

3: 95 percent / LAH / tetrahydrofuran / 31 h / 0 - 20 °C

4: 230 mg / pyridine / 12 h / 20 °C

With pyridine; lithium aluminium tetrahydride; 4-pyrrolidin-1-ylpyridine; In tetrahydrofuran; toluene;
DOI:10.1039/b109396g

Reference yield:

: 438569-46-1
2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-ol

: 438569-49-4
Oxo-phenyl-acetic acid (R)-2,2-dimethyl-7-(2,4,6-trimethyl-phenyl)-indan-1-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 794 mg / 4-pyrrolidinopyridine; pyridine / toluene / 12 h / Heating

2: 95 percent / LAH / tetrahydrofuran / 31 h / 0 - 20 °C

3: 230 mg / pyridine / 12 h / 20 °C

With pyridine; lithium aluminium tetrahydride; 4-pyrrolidin-1-ylpyridine; In tetrahydrofuran; toluene;
DOI:10.1039/b109396g