C₁₄H₂₀N₂O₇

Base Information

• Chemical Name: C₁₄H₂₀N₂O₇
• CAS No.: 1446093-37-3
• Molecular Formula: C₁₄H₂₀N₂O₇
• Molecular Weight: 328.322
• Mol file: 1446093-37-3.mol

Synonyms:

Chemical Property of C₁₄H₂₀N₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀N₂O₇

There total 4 articles about C₁₄H₂₀N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl-6-chlor-6-deoxy-α-D-mannopyranosid (4990-80-1) → C14H20N2O7 (1446093-37-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 4 h / 70 °C

2: palladium on activated charcoal; hydrogen / ethanol / 12 h / 20 °C

3: sodium tetrahydroborate / 12 h

With sodium tetrahydroborate; sodium azide; palladium on activated charcoal; hydrogen; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/cb400371r

Reference yield:

(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol (617-04-9) → C14H20N2O7 (1446093-37-3)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine; p-toluenesulfonyl chloride / 24 h / 20 °C

2: sodium azide / N,N-dimethyl-formamide / 4 h / 70 °C

3: palladium on activated charcoal; hydrogen / ethanol / 12 h / 20 °C

4: sodium tetrahydroborate / 12 h

With pyridine; sodium tetrahydroborate; sodium azide; palladium on activated charcoal; hydrogen; p-toluenesulfonyl chloride; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/cb400371r

Reference yield:

methyl 6-azido-6-deoxy-α-D-mannopyranoside (66224-56-4) → C14H20N2O7 (1446093-37-3)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / ethanol / 12 h / 20 °C

2: sodium tetrahydroborate / 12 h

With sodium tetrahydroborate; palladium on activated charcoal; hydrogen; In ethanol;

DOI:10.1021/cb400371r

upstream raw materials:

methyl 6-amino-6-deoxy-α-D-mannopyrannoside

4-nitrobenzaldehdye

Methyl-6-chlor-6-deoxy-α-D-mannopyranosid

(2R,3S,4S,5S,6S)-2-(hydroxymethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol

Refernces