C₃₃H₃₃N₃O₂SSe

Base Information

Chemical Name:C₃₃H₃₃N₃O₂SSe
CAS No.:1559062-39-3
Molecular Formula:C₃₃H₃₃N₃O₂SSe
Molecular Weight:614.67
Hs Code.:

C<sub>33</sub>H<sub>33</sub>N<sub>3</sub>O<sub>2</sub>SSe

Synonyms:

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Chemical Property of C₃₃H₃₃N₃O₂SSe

Chemical Property:

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Technology Process of C₃₃H₃₃N₃O₂SSe

There total 6 articles about C₃₃H₃₃N₃O₂SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130-95-0
quinine

: 1559062-39-3
C₃₃H₃₃N₃O₂SSe

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

1.2: 4 h / 0 - 5 °C

2.1: sodium azide / N,N-dimethyl-formamide / 20 h / 60 °C

3.1: triphenylphosphine / tetrahydrofuran / 4 h / 60 °C

3.2: 10 h / 20 °C

4.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

5.1: potassium tert-butoxyselenolate / N,N-dimethyl-formamide / 20 h / 110 °C

6.1: d⁽⁴⁾-methanol

With sodium azide; potassium tert-butoxyselenolate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; d⁽⁴⁾-methanol; N,N-dimethyl-formamide; 3.1: |Staudinger Azide Reduction;
DOI:10.1039/c4ob00027g

Reference yield:

: 249731-47-3
quinine 9O-methanesulfonate

: 1559062-39-3
C₃₃H₃₃N₃O₂SSe

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide / N,N-dimethyl-formamide / 20 h / 60 °C

2.1: triphenylphosphine / tetrahydrofuran / 4 h / 60 °C

2.2: 10 h / 20 °C

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: potassium tert-butoxyselenolate / N,N-dimethyl-formamide / 20 h / 110 °C

5.1: d⁽⁴⁾-methanol

With sodium azide; potassium tert-butoxyselenolate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; d⁽⁴⁾-methanol; N,N-dimethyl-formamide; 2.1: |Staudinger Azide Reduction;
DOI:10.1039/c4ob00027g

Reference yield:

: 9-epi-9-amino-9-deoxyquinine

: 1559062-39-3
C₃₃H₃₃N₃O₂SSe

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

2: potassium tert-butoxyselenolate / N,N-dimethyl-formamide / 20 h / 110 °C

3: d⁽⁴⁾-methanol

With potassium tert-butoxyselenolate; triethylamine; In dichloromethane; d⁽⁴⁾-methanol; N,N-dimethyl-formamide;
DOI:10.1039/c4ob00027g