Technology Process of C12H15(2)HO
There total 5 articles about C12H15(2)HO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 0.166667h;
Ambient temperature;
DOI:10.1021/ja00348a030
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 39 percent / n-butyllithium, deuterium oxide / hexane; tetrahydrofuran / 1 h / Ambient temperature
2: 44 percent / n-butyllithium, water / hexane; tetrahydrofuran
3: 26 percent / CH2Cl2 / 60 h / Heating
4: 75 percent / sodium amalgam, methanol, disodium hydrogen phosphate / tetrahydrofuran / Ambient temperature
5: 73 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.17 h / Ambient temperature
With
methanol; disodium hydrogenphosphate; sodium amalgam; n-butyllithium; water; water-d2; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja00348a030
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 26 percent / CH2Cl2 / 60 h / Heating
2: 75 percent / sodium amalgam, methanol, disodium hydrogen phosphate / tetrahydrofuran / Ambient temperature
3: 73 percent / m-chloroperbenzoic acid / CH2Cl2 / 0.17 h / Ambient temperature
With
methanol; disodium hydrogenphosphate; sodium amalgam; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00348a030
