tetrakis(2-anilinopyridine)ditungsten(II)*2/3THF

Base Information

• Chemical Name: tetrakis(2-anilinopyridine)ditungsten(II)*2/3THF
• CAS No.: 93110-48-6
• Molecular Formula: 0C₄H₈O*C₄₄H₃₆N₈W₂
• Molecular Weight: 1092.84

Synonyms:

Chemical Property of tetrakis(2-anilinopyridine)ditungsten(II)*2/3THF

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Technology Process of tetrakis(2-anilinopyridine)ditungsten(II)*2/3THF

There total 1 articles about tetrakis(2-anilinopyridine)ditungsten(II)*2/3THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lithium N-phenyl(2-pyridyl) amide + tungsten(IV) chloride (13470-13-8) → tetrakis(2-anilinopyridine)ditungsten(II)*2/3THF (93110-48-6)

Guidance literature:

With Na#Hg; In tetrahydrofuran; WCl4 was dissolved in THF, at -40°C Na#Hg was added, stirred for30 min, until the temp. reached -20°C, LiPhNpy in THF was transferred to THF soln., mixt. was allowed to warm to room temp., stirred overnight; filtered, mixed with toluene, covered with hexane;

upstream raw materials:

tungsten(IV) chloride

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