bis(trifluoromethyl)arsinophosphazene

Base Information

Chemical Name:bis(trifluoromethyl)arsinophosphazene
CAS No.:148146-50-3
Molecular Formula:C₂₀H₁₅AsF₆NP
Molecular Weight:489.232
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(trifluoromethyl)arsinophosphazene

Chemical Property:

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Technology Process of bis(trifluoromethyl)arsinophosphazene

There total 1 articles about bis(trifluoromethyl)arsinophosphazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: bis(trifluoromethyl)arsinous azide

: 603-35-0
triphenylphosphine

: 148146-50-3
bis(trifluoromethyl)arsinophosphazene

Guidance literature:: In dichloromethane; for 1.33333h; Ambient temperature;
DOI:10.1039/DT9930000663

Reference yield: 70.0%

: 133869-39-3,65702-94-5
undecacarbonyl(acetonitrile)triosmium

: 148146-50-3
bis(trifluoromethyl)arsinophosphazene

: 148537-32-0
{Os₃(CO)11((CF₃)2AsNP(C₆H₅)3)}

Guidance literature:: In dichloromethane; react. of arsinophosphazene and carbonyl complex at room temp., 24h, formation of a bright yellow soln.;; concg.; TLC (eluent CH2Cl2-hexane=1:9); extraction of an intense yellow band and recrytn. from CH2Cl2-hexane; elem. anal.;;
DOI:10.1039/DT9930000663

Reference yield: 31.0%

: decacarbonyltriosmiumdihydride

: 148146-50-3
bis(trifluoromethyl)arsinophosphazene

: {Os₃(CO)9(H)2((CF₃)2AsNP(C₆H₅)3)}

Guidance literature:: In dichloromethane; react. of arsinophosphazene and carbonyl complex at 80°C, 6h, evacuated tube; color change at the end of react. from purplish to wine-red;; concg.; TLC (eluent CH2Cl2-hexane=1:9); extraction of an intense purplish band and recrytn. from CH2Cl2-hexane; elem. anal.;;
DOI:10.1039/DT9930000663