6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,13,15⁽³⁰⁾,25⁽²⁹⁾,26-hexaene-3,9,17,23-tetracarbonitrile

Base Information

• Chemical Name: 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,13,15⁽³⁰⁾,25⁽²⁹⁾,26-hexaene-3,9,17,23-tetracarbonitrile
• CAS No.: 1027162-60-2
• Molecular Formula: C₄₂H₄₆N₁₀O₄S₂
• Molecular Weight: 819.024

Synonyms:

Chemical Property of 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,13,15⁽³⁰⁾,25⁽²⁹⁾,26-hexaene-3,9,17,23-tetracarbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,13,15⁽³⁰⁾,25⁽²⁹⁾,26-hexaene-3,9,17,23-tetracarbonitrile

There total 5 articles about 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.1^11,15]triaconta-1⁽²⁸⁾,11,13,15⁽³⁰⁾,25⁽²⁹⁾,26-hexaene-3,9,17,23-tetracarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.111,15]triaconta-1(28),11,13,15(30),25(29),26-hexaene-3,9,17,23-tetracarbonitrile (1027162-60-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 78 percent / pyridine / 1.) 0 deg C, 3 h, 2.) room temperature, 2 h

2: B₂H₆ / tetrahydrofuran / 20 h / Heating

3: 87 percent / acetonitrile / 24 h / Ambient temperature

4: dimethylsulfoxide; ethanol / 5 h / Heating

With pyridine; diborane; In tetrahydrofuran; ethanol; dimethyl sulfoxide; acetonitrile;

DOI:10.1039/a700937b

Reference yield:

N,N-Bis-cyanomethyl-4-methyl-benzenesulfonamide (198954-96-0) → 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.111,15]triaconta-1(28),11,13,15(30),25(29),26-hexaene-3,9,17,23-tetracarbonitrile (1027162-60-2)

Guidance literature:

Multi-step reaction with 3 steps

1: B₂H₆ / tetrahydrofuran / 20 h / Heating

2: 87 percent / acetonitrile / 24 h / Ambient temperature

3: dimethylsulfoxide; ethanol / 5 h / Heating

With diborane; In tetrahydrofuran; ethanol; dimethyl sulfoxide; acetonitrile;

DOI:10.1039/a700937b

Reference yield:

(2E,9E,16E,23E)-6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.111,15]triaconta-1(28),2,9,11,13,15(30),16,23,25(29),26-decaene → 6,20-Bis-(toluene-4-sulfonyl)-3,6,9,17,20,23-hexaaza-tricyclo[23.3.1.111,15]triaconta-1(28),11,13,15(30),25(29),26-hexaene-3,9,17,23-tetracarbonitrile (1027162-60-2)

Guidance literature:

In ethanol; dimethyl sulfoxide; for 5h; Heating;

DOI:10.1039/a700937b

upstream raw materials:

Isophthalaldehyde

N,N-bis(2-aminoethyl)-4-methyl-benzenesulfonamide

p-toluenesulfonyl chloride

N,N-Bis-cyanomethyl-4-methyl-benzenesulfonamide

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