14-hydroxy-3β-(O⁴-{O⁴-[(7S)-4-(4-hydroxy-phenethyl)-2c-methyl-[1,4]oxazepan-7r-yl]-β-D-ribo-2,6-dideoxy-hexopyranosyl}-β-D-ribo-2,6-dideoxy-hexopyranosyloxy)-(5β,14β)-card-20(22)-enolide

Base Information

• Chemical Name: 14-hydroxy-3β-(O⁴-{O⁴-[(7S)-4-(4-hydroxy-phenethyl)-2c-methyl-[1,4]oxazepan-7r-yl]-β-D-ribo-2,6-dideoxy-hexopyranosyl}-β-D-ribo-2,6-dideoxy-hexopyranosyloxy)-(5β,14β)-card-20(22)-enolide
• CAS No.: 70833-92-0
• Molecular Formula: C₄₉H₇₃NO₁₂
• Molecular Weight: 868.118

Synonyms:

Chemical Property of 14-hydroxy-3β-(O⁴-{O⁴-[(7S)-4-(4-hydroxy-phenethyl)-2c-methyl-[1,4]oxazepan-7r-yl]-β-D-ribo-2,6-dideoxy-hexopyranosyl}-β-D-ribo-2,6-dideoxy-hexopyranosyloxy)-(5β,14β)-card-20(22)-enolide

Chemical Property:

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Technology Process of 14-hydroxy-3β-(O⁴-{O⁴-[(7S)-4-(4-hydroxy-phenethyl)-2c-methyl-[1,4]oxazepan-7r-yl]-β-D-ribo-2,6-dideoxy-hexopyranosyl}-β-D-ribo-2,6-dideoxy-hexopyranosyloxy)-(5β,14β)-card-20(22)-enolide

There total 1 articles about 14-hydroxy-3β-(O⁴-{O⁴-[(7S)-4-(4-hydroxy-phenethyl)-2c-methyl-[1,4]oxazepan-7r-yl]-β-D-ribo-2,6-dideoxy-hexopyranosyl}-β-D-ribo-2,6-dideoxy-hexopyranosyloxy)-(5β,14β)-card-20(22)-enolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tyramine hydrochloride (60-19-5) + digitoxin-dialdehyde (70877-95-1) → 14-hydroxy-3β-(O4-{O4-[(7S)-4-(4-hydroxy-phenethyl)-2c-methyl-[1,4]oxazepan-7r-yl]-β-D-ribo-2,6-dideoxy-hexopyranosyl}-β-D-ribo-2,6-dideoxy-hexopyranosyloxy)-(5β,14β)-card-20(22)-enolide (70833-92-0)

Guidance literature:

With sodium cyanoborohydride; In methanol; Ambient temperature;

DOI:10.1002/jlcr.2580150127

upstream raw materials:

tyramine hydrochloride

digitoxin-dialdehyde

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