5--1-<4-amino-2-methoxy-phenoxy>-pentan

Base Information

• Chemical Name: 5--1-<4-amino-2-methoxy-phenoxy>-pentan
• CAS No.: 593266-74-1
• Molecular Formula: C₃₉H₆₃NO₂S
• Molecular Weight: 610.001

Synonyms:

Chemical Property of 5--1-<4-amino-2-methoxy-phenoxy>-pentan

Chemical Property:

Purity/Quality:

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Technology Process of 5--1-<4-amino-2-methoxy-phenoxy>-pentan

There total 3 articles about 5--1-<4-amino-2-methoxy-phenoxy>-pentan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1--5-(4-nitro-2-methoxy-phenoxy)-pentan (96872-92-3) → 5--1-<4-amino-2-methoxy-phenoxy>-pentan (593266-74-1)

Guidance literature:

With sodium sulfide; In 2-ethoxy-ethanol; at 100 ℃;

DOI:10.1039/jr9620000178

Reference yield:

α-Bromo-ω-(2-methoxy-4-nitrophenoxy)pentane (100141-12-6) → 5--1-<4-amino-2-methoxy-phenoxy>-pentan (593266-74-1)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOEt / ethanol

2: Na₂S / 2-ethoxy-ethanol / 100 °C

With sodium sulfide; sodium ethanolate; In 2-ethoxy-ethanol; ethanol;

DOI:10.1039/jr9620000178

Reference yield:

thiocholesterol (1249-81-6) → 5--1-<4-amino-2-methoxy-phenoxy>-pentan (593266-74-1)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOEt / ethanol

2: Na₂S / 2-ethoxy-ethanol / 100 °C

With sodium sulfide; sodium ethanolate; In 2-ethoxy-ethanol; ethanol;

DOI:10.1039/jr9620000178

upstream raw materials:

1--5-(4-nitro-2-methoxy-phenoxy)-pentan

α-Bromo-ω-(2-methoxy-4-nitrophenoxy)pentane

thiocholesterol

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