Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

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Chemical Name:Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside
CAS No.:172945-34-5
Molecular Formula:C₇₂H₉₆N₂O₂₄
Molecular Weight:1373.55
Hs Code.:

Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

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Chemical Property of Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

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Technology Process of Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

There total 10 articles about Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 162019-62-7
Methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-2-O-<3-(methylthiomethoxy)propyl>-α-D-neuraminate

: 172945-32-3
Hexyl 2-acetamido-6-O-benzyl-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-deoxy-β-D-glucopyranoside

: 172945-34-5
Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; molecular sieve; trifluorormethanesulfonic acid; In 1,4-dioxane; dichloromethane; 1.) 30 min, 2.) 2 h;
DOI:10.1002/recl.19951140905

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 172945-34-5
Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: p-TsOH / dimethylformamide / 4 h

2: IDCP, molecular sieves / CH₂Cl₂; diethyl ether / 1.) 45 min, 2.) 1 h

3: 59 percent / Me₃N*BH₃, AlCl₃, molecular sieves / tetrahydrofuran / 16 h

4: 59 percent / molecular sieves, NIS, TfOH / CH₂Cl₂; dioxane / 1.) 30 min, 2.) 2 h

With N-iodo-succinimide; aluminium trichloride; molecular sieve; trifluorormethanesulfonic acid; iodonium(di-γ-collidine) perchlorate; trimethylamine-borane; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/recl.19951140905

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyranoso)[1,2-d]-2-oxazoline

: 172945-34-5
Hexyl 2-acetamido-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-<3-<(methyl 4,7,8,9-tetra-O-acetyl-N-acetyl-α-D-neuraminate-2-yl)oxy>propoxymethyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 74 percent / TfOH / CH₂Cl₂ / 2 h

2: NaOMe / methanol / 2 h

3: p-TsOH / dimethylformamide / 4 h

4: IDCP, molecular sieves / CH₂Cl₂; diethyl ether / 1.) 45 min, 2.) 1 h

5: 59 percent / Me₃N*BH₃, AlCl₃, molecular sieves / tetrahydrofuran / 16 h

6: 59 percent / molecular sieves, NIS, TfOH / CH₂Cl₂; dioxane / 1.) 30 min, 2.) 2 h

With N-iodo-succinimide; aluminium trichloride; molecular sieve; trifluorormethanesulfonic acid; iodonium(di-γ-collidine) perchlorate; trimethylamine-borane; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/recl.19951140905