(N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate

Base Information

Chemical Name:(N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate
CAS No.:528572-76-1
Molecular Formula:CF₃O₃S*C₄₈H₄₅N₂O₄P₂Ru
Molecular Weight:1025.98
Hs Code.:

(N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate

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Chemical Property of (N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate

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Technology Process of (N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate

There total 1 articles about (N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 260266-16-8,364622-30-0,133519-04-7,134527-17-6
(6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane))2Ru(OC(O)CH₃)2

: 1493-13-6
trifluorormethanesulfonic acid

: 140-50-1
N,N'-diacetyl-1,4-phenylenediamine

: 528572-76-1
(N-[4-(N-acetylamino)-η6-phenyl]acetamide)[6,6'-dimethoxybiphenyl-2,2'-diylbis(diphenylphosphane)-κ2P,P']hydridoruthenium(II) trifluoromethanesulfonate

Guidance literature:: In isopropyl alcohol; heating a suspn. of Ru complex and arene in isopropanol to 75°C, treating with CF3SO3H; cooling to room temp., concg. in vac., pptn. by addn. of pentane, filtration, washing with diethyl ether, drying; elem. anal.;
DOI:10.1002/1522-2675(200211)85:11<3937::AID-HLCA3937>3.0.CO;2-X