tetracarbonyl(4-[(pyridin-2-ylmethylene)amino]phenol)chromium

Base Information

• Chemical Name: tetracarbonyl(4-[(pyridin-2-ylmethylene)amino]phenol)chromium
• CAS No.: 452322-78-0
• Molecular Formula: C₁₆H₁₀CrN₂O₅
• Molecular Weight: 362.262
• Mol file: 452322-78-0.mol

Synonyms:

Chemical Property of tetracarbonyl(4-[(pyridin-2-ylmethylene)amino]phenol)chromium

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tetracarbonyl(4-[(pyridin-2-ylmethylene)amino]phenol)chromium

There total 1 articles about tetracarbonyl(4-[(pyridin-2-ylmethylene)amino]phenol)chromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(4-hydroxyphenyl)(pyridin-2-ylmethylene)amine (13160-68-4) + tetracarbonylbis(acetonitrile)chromium (16800-44-5,29890-09-3) → tetracarbonyl(4-[(pyridin-2-ylmethylene)amino]phenol)chromium (452322-78-0)

Guidance literature:

In tetrahydrofuran; under Ar, standard Schlenk techniques; solid ligand added to soln. of Crcomplex (molar ratio 1:1) in THF; similarly to K. Heinze, J. Chem. Soc. , Dalton Trans., 2002, 540-547; evapd. to dryness; filtered through pad of kieselgur (THF); vol. of the soln. reduced; layered with PE40/60; filtered; ppt. dried in vac.; recrystd. from acetone and PE40/60; elem. anal.;

DOI:10.1039/b201647h

upstream raw materials:

(4-hydroxyphenyl)(pyridin-2-ylmethylene)amine

tetracarbonylbis(acetonitrile)chromium