2-carbomethoxy-4,6-dimethoxybenzophenone

Base Information

Chemical Name:2-carbomethoxy-4,6-dimethoxybenzophenone
CAS No.:90685-28-2
Molecular Formula:C₁₇H₁₆O₅
Molecular Weight:301.3
Hs Code.:

2-carbomethoxy-4,6-dimethoxy<carbonyl-13C>benzophenone

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-carbomethoxy-4,6-dimethoxybenzophenone

Chemical Property:

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Technology Process of 2-carbomethoxy-4,6-dimethoxybenzophenone

There total 1 articles about 2-carbomethoxy-4,6-dimethoxybenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52947-05-4
[α-13C]benzoyl chloride

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 90685-28-2
2-carbomethoxy-4,6-dimethoxybenzophenone

Guidance literature:: With aluminium trichloride; for 24h; Ambient temperature;
DOI:10.1016/S0031-9422(00)80323-4

Reference yield:

: 90685-28-2
2-carbomethoxy-4,6-dimethoxybenzophenone

: 90685-29-3
2-carbomethoxy-4,6-dimethoxydiphenylmethane

Guidance literature:: With triethylsilane; In trifluoroacetic acid; for 48h; Ambient temperature;
DOI:10.1016/S0031-9422(00)80323-4

Reference yield:

: 90685-28-2
2-carbomethoxy-4,6-dimethoxybenzophenone

: 90685-30-6
2-carboxy-4,6-dimethoxydiphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1: 320 mg / Et₃SiH / trifluoroacetic acid / 48 h / Ambient temperature

2: 280 mg / 2M NaOH / methanol; H₂O / 3 h / Heating

With triethylsilane; sodium hydroxide; In methanol; water; trifluoroacetic acid;
DOI:10.1016/S0031-9422(00)80323-4