Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate

Base Information

Chemical Name:Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate
CAS No.:4550-93-0
Molecular Formula:C₃₆H₃₆O₈
Molecular Weight:596.677
Hs Code.:
Mol file:4550-93-0.mol

Synonyms:

Suppliers and Price of Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate
50mg
$ 460.00

TRC
Benzyl2,3,4-Tri-O-benzyl-D-glucuronateAcetate
100mg
$ 595.00

Medical Isotopes, Inc.
Benzyl2,3,4-Tri-O-benzyl-D-glucuronateAcetate
50 mg
$ 650.00

Total 4 raw suppliers

Chemical Property of Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate is a reactant in the preparation of bile acid 24-acyl glucuronides.

Technology Process of Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate

There total 8 articles about Benzyl 2,3,4-Tri-O-benzyl-D-glucuronate Acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2595-06-4,18685-19-3,40653-13-2,40653-30-3,67583-56-6,68027-26-9,73111-52-1
methyl 2,3,4-tri-O-benzyl-6-O-trityl-α-D-glucopyranoside

: 4550-93-0,93527-89-0,111613-22-0
(2S,3S,4S,5R,6R)-6-Acetoxy-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85.3 percent / conc. H₂SO₄ / ethanol / 3 h / Ambient temperature

2: CrO₃, H₂SO₄ / acetone / 0.5 h / Ambient temperature

3: NaHCO₃ / dimethylsulfoxide / 8 h / Ambient temperature

4: AcOH, H₂SO₄ / 5 h / Ambient temperature

With chromium(VI) oxide; sulfuric acid; sodium hydrogencarbonate; acetic acid; In ethanol; dimethyl sulfoxide; acetone;
DOI:10.1016/S0039-128X(97)00160-8

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 4550-93-0,93527-89-0,111613-22-0
(2S,3S,4S,5R,6R)-6-Acetoxy-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CrO₃, H₂SO₄ / acetone / 0.5 h / Ambient temperature

2: NaHCO₃ / dimethylsulfoxide / 8 h / Ambient temperature

3: AcOH, H₂SO₄ / 5 h / Ambient temperature

With chromium(VI) oxide; sulfuric acid; sodium hydrogencarbonate; acetic acid; In dimethyl sulfoxide; acetone;
DOI:10.1016/S0039-128X(97)00160-8

Reference yield:

: 120444-48-6
(2S,3S,4S,5R,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-carboxylic acid

: 4550-93-0,93527-89-0,111613-22-0
(2S,3S,4S,5R,6R)-6-Acetoxy-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / dimethylsulfoxide / 8 h / Ambient temperature

2: AcOH, H₂SO₄ / 5 h / Ambient temperature

With sulfuric acid; sodium hydrogencarbonate; acetic acid; In dimethyl sulfoxide;
DOI:10.1016/S0039-128X(97)00160-8