[[[[(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methoxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl] [(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methyl hydrogen phosphate

Base Information

• Chemical Name: [[[[(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methoxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl] [(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methyl hydrogen phosphate
• CAS No.: 117137-55-0
• Molecular Formula: C₂₀H₂₈N₁₀O₁₉P₄
• Molecular Weight: 836.393

Synonyms:

Chemical Property of [[[[(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methoxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl] [(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methyl hydrogen phosphate

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Technology Process of [[[[(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methoxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl] [(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methyl hydrogen phosphate

There total 16 articles about [[[[(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methoxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl]oxy-hydroxy-phosphoryl] [(2R,3S,4R,5R)-5-(6-aminopurin-9-yl)-3,4-dihydroxy-tetrahydrofuran-2-yl]methyl hydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ATP (56-65-5,896506-78-8) → Diadenosine tetraphosphate (5542-28-9,117137-55-0)

Guidance literature:

With LEUCINE; In various solvent(s); at 40 ℃; at pH 7.5; ATP-regenerating system of acetate kinase, adenylate kinase, PPase with acetyl phosphate;

Reference yield: 90.0%

α,β-methylene-guanosine 5'-triphosphate sodium salt + adenosine 5'-triphosphate sodium salt (4691-96-7) → AppCH2ppG sodium salt + Diadenosine triphosphate (5959-90-0,158700-26-6) + Diadenosine tetraphosphate (5542-28-9,117137-55-0)

Guidance literature:

With L-lysine; pyrophosphatase; In water; at 38 ℃; pH=8.0; Tris-HCl-buffer; Enzymatic reaction;

Reference yield: 75.0%

adenosine 5'-phosphorimidazolide (20816-58-4,116273-87-1) + ATP (56-65-5,896506-78-8) → Diadenosine tetraphosphate (5542-28-9,117137-55-0)

Guidance literature:

With H₉₆F-Fhit; magnesium chloride; In various solvent(s); at 20 ℃; for 1h; pH=5.5;

DOI:10.1021/ja0400640

upstream raw materials:

adenosine 5'-trimetaphosphate

tris(tributylammonio)-ADP

ATP

C₁₉H₁₉ClN₆O₁₀P₂

Downstream raw materials:

adenosine 5'-diphosphate

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